SYNTHESIS OF 3-NITRO-N-(1, 1, 3-TRIOXO-1,3-DIHYDRO-2H- 1λ6,2-BENZOTHIAZOLE-2-CARBOTHIOYL)BENZAMIDE

• Autores: Angulo-Cornejo, Jorge R., Ceroni-Galloso, Mario, Lino-Pacheco, María N., Villanueva-Huerta, Claudia C., Tovar-Taboada, Carlo Felipe
• Formato: artículo
• Fecha de Publicación: 2017
• Institución: Sociedad Química del Perú
• Repositorio: Revista de la Sociedad Química del Perú
• Lenguaje: español
• OAI Identifier: oai:rsqp.revistas.sqperu.org.pe:article/148
• Enlace del recurso: http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/148
• Nivel de acceso: acceso abierto
• Materia: Benzoylthiourea; Saccharin; 3-Nitro benzoyl; Ligand N; S; O donor; Benzoiltiourea; Sacarina; 3-Nitro-benzoil; Ligando N; O dador

The novel compound 3-nitro-N-(1, 1, 3-trioxo-1, 3-dihydro-2H-1λ6, 2-benzothiazole-2- carbothioyl)benzamide has been synthesized and is characterized by elemental analysis, infrared spectroscopy, nuclear magnetic resonance 1H and 13C. The structure of the new compound shows a characteristic signal in the 1H-NMR spectrum of the NH group to fields highly displaced by the presence of a highly deprotected hydrogen at 11.90 ppm, due to the existence of a hydrogen bond between the C = O of saccharin group and the NH group.