OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT

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In the present study, the ethanolic and aqueous extracts of the leaves of Annona muricata L. were obtained. The extraction conditions were established from the total soluble solids content and the corrosion inhibiting effect obtained from the polarization resistance, Rp (Ω • cm2), of the steel 1008,...

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Detalles Bibliográficos
Autores: Vergara Sotomayor, Abel, Páucar Cuba, Karín, Morales Comettant, Carlos, Castro Mandujano, Olivio, Pizarro Solís, Pedro, Díaz Rosado, José
Formato: artículo
Fecha de Publicación:2018
Institución:Sociedad Química del Perú
Repositorio:Revista de la Sociedad Química del Perú
Lenguaje:español
OAI Identifier:oai:rsqp.revistas.sqperu.org.pe:article/173
Enlace del recurso:http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/173
Nivel de acceso:acceso abierto
Materia:Annona muricata
extract
alkaloids
carbon steel
extracto
alcaloides
carbón steel
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spelling OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECTOBTENCIÓN DE EXTRACTOS DE HOJAS DE Annona muricata L. (GUANÁBANA) INDUCIDOS POR SU EFECTO INHIBIDOR DE LA CORROSIÓNVergara Sotomayor, AbelPáucar Cuba, KarínMorales Comettant, CarlosCastro Mandujano, OlivioPizarro Solís, PedroDíaz Rosado, JoséAnnona muricataextractalkaloidscarbon steelAnnona muricataextractoalcaloidescarbón steelIn the present study, the ethanolic and aqueous extracts of the leaves of Annona muricata L. were obtained. The extraction conditions were established from the total soluble solids content and the corrosion inhibiting effect obtained from the polarization resistance, Rp (Ω • cm2), of the steel 1008, in a 1 Molar solution of HCl in the absence and presence of the inhibitor extract. The extracts with greater corrosion inhibiting effect were characterized by phytochemical screening, quantification of total phenols, alkaloids, flavonoids and antioxidant activity (DPPH). The ethanolic extract had a 1.5 times greater corrosion inhibiting effect than the aqueous extract. The phytochemical screening established that both extracts contain a wide variety of secondary metabolites, such as phenols, alkaloids, flavonoids, tannins and sesquiterpenoid lactones. Among the studied extracts, the ethanolic extract had the highest content in total phenols (582.99 and 523.34 μg EAG / mL EE), alkaloids (3.76 and 1.52 % lupanin) and flavonoids (1.14 and 0.76 mg quercetin/mL of extract), but the lowest antioxidant activity (91.45 and 94.93 % of DPPH). The images obtained by SEM and the EDS analysis for the steel exposed to the acid solution in the absence and presence of the inhibitor extract showed its protective against corrosion.En el presente estudio fueron obtenidos los extractos etanólico y acuoso de las hojas de Annona muricata L. Las condiciones de extracción se establecieron a partir del contenido de sólidos solubles totales y el efecto inhibidor de la corrosión obtenido a partir de la resistencia a la polarización, Rp (Ω•cm2), del acero 1008 en una solución de HCl 1M en ausencia y presencia del extracto inhibidor. Los extractos con mayor efecto inhibidor de corrosión fueron caracterizados por tamizaje fitoquímico, cuantificación de fenoles totales, alcaloides, flavonoides y actividad antioxidante (DPPH). El extracto etanólico presentó un efecto inhibidor de la corrosión 1,5 veces mayor que el extracto acuoso. El tamizaje fitoquímico estableció que ambos extractos contienen principalmente fenoles, alcaloides, flavonoides, taninos y lactonas sesquiterpenoides. Entre los extractos estudiados, el extracto etanólico presentó el mayor contenido en fenoles totales (582,99 y 523,34 μg EAG /mL EE), alcaloides (3,76 y 1,52 % lupanina) y flavonoides (1,14 y 0,76 mg quercetina/mL de extracto), pero la menor actividad antioxidante (91,45 y 94,93 % de DPPH). Las imágenes obtenidas por SEM y el análisis EDS para el acero expuesto a la solución ácida en ausencia y presencia del extracto inhibidor evidenciaron su carácter protector contra la corrosión.Sociedad Química del Perú2018-03-31info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontexttextoapplication/pdfhttp://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/17310.37761/rsqp.v84i1.173Revista de la Sociedad Química del Perú; Vol. 84 Núm. 1 (2018): Revista de la Sociedad Química del Perú; 119 - 132Journal of the Chemical Society of Peru; Vol. 84 No. 1 (2018): Journal of Sociedad Química del Perú; 119 - 1322309-87401810-634X10.37761/rsqp.v84i1reponame:Revista de la Sociedad Química del Perúinstname:Sociedad Química del Perúinstacron:SQPspahttp://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/173/14720182018Derechos de autor 2018 Sociedad Química del Perúhttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessoai:rsqp.revistas.sqperu.org.pe:article/1732020-03-03T22:16:47Z
dc.title.none.fl_str_mv OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
OBTENCIÓN DE EXTRACTOS DE HOJAS DE Annona muricata L. (GUANÁBANA) INDUCIDOS POR SU EFECTO INHIBIDOR DE LA CORROSIÓN
title OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
spellingShingle OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
Vergara Sotomayor, Abel
Annona muricata
extract
alkaloids
carbon steel
Annona muricata
extracto
alcaloides
carbón steel
title_short OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
title_full OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
title_fullStr OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
title_full_unstemmed OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
title_sort OBTAINING AND PHYTOCHEMICAL STUDY OF EXTRACTS OF Annona muricata (GUANÁBANA) INDUCED BY ITS CORROSION INHIBITING EFFECT
dc.creator.none.fl_str_mv Vergara Sotomayor, Abel
Páucar Cuba, Karín
Morales Comettant, Carlos
Castro Mandujano, Olivio
Pizarro Solís, Pedro
Díaz Rosado, José
author Vergara Sotomayor, Abel
author_facet Vergara Sotomayor, Abel
Páucar Cuba, Karín
Morales Comettant, Carlos
Castro Mandujano, Olivio
Pizarro Solís, Pedro
Díaz Rosado, José
author_role author
author2 Páucar Cuba, Karín
Morales Comettant, Carlos
Castro Mandujano, Olivio
Pizarro Solís, Pedro
Díaz Rosado, José
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv Annona muricata
extract
alkaloids
carbon steel
Annona muricata
extracto
alcaloides
carbón steel
topic Annona muricata
extract
alkaloids
carbon steel
Annona muricata
extracto
alcaloides
carbón steel
description In the present study, the ethanolic and aqueous extracts of the leaves of Annona muricata L. were obtained. The extraction conditions were established from the total soluble solids content and the corrosion inhibiting effect obtained from the polarization resistance, Rp (Ω • cm2), of the steel 1008, in a 1 Molar solution of HCl in the absence and presence of the inhibitor extract. The extracts with greater corrosion inhibiting effect were characterized by phytochemical screening, quantification of total phenols, alkaloids, flavonoids and antioxidant activity (DPPH). The ethanolic extract had a 1.5 times greater corrosion inhibiting effect than the aqueous extract. The phytochemical screening established that both extracts contain a wide variety of secondary metabolites, such as phenols, alkaloids, flavonoids, tannins and sesquiterpenoid lactones. Among the studied extracts, the ethanolic extract had the highest content in total phenols (582.99 and 523.34 μg EAG / mL EE), alkaloids (3.76 and 1.52 % lupanin) and flavonoids (1.14 and 0.76 mg quercetin/mL of extract), but the lowest antioxidant activity (91.45 and 94.93 % of DPPH). The images obtained by SEM and the EDS analysis for the steel exposed to the acid solution in the absence and presence of the inhibitor extract showed its protective against corrosion.
publishDate 2018
dc.date.none.fl_str_mv 2018-03-31
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
text
texto
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/173
10.37761/rsqp.v84i1.173
url http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/173
identifier_str_mv 10.37761/rsqp.v84i1.173
dc.language.none.fl_str_mv spa
language spa
dc.relation.none.fl_str_mv http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/173/147
dc.rights.none.fl_str_mv Derechos de autor 2018 Sociedad Química del Perú
https://creativecommons.org/licenses/by/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Derechos de autor 2018 Sociedad Química del Perú
https://creativecommons.org/licenses/by/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.coverage.none.fl_str_mv 2018
2018
dc.publisher.none.fl_str_mv Sociedad Química del Perú
publisher.none.fl_str_mv Sociedad Química del Perú
dc.source.none.fl_str_mv Revista de la Sociedad Química del Perú; Vol. 84 Núm. 1 (2018): Revista de la Sociedad Química del Perú; 119 - 132
Journal of the Chemical Society of Peru; Vol. 84 No. 1 (2018): Journal of Sociedad Química del Perú; 119 - 132
2309-8740
1810-634X
10.37761/rsqp.v84i1
reponame:Revista de la Sociedad Química del Perú
instname:Sociedad Química del Perú
instacron:SQP
instname_str Sociedad Química del Perú
instacron_str SQP
institution SQP
reponame_str Revista de la Sociedad Química del Perú
collection Revista de la Sociedad Química del Perú
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 13.121034
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