XRF elemental analysis of inks in South American manuscripts from 1779 to 1825
Descripción del Articulo
This work was carried out with resources from the gas canon of the Cusco Region and the support of FONDECYT—CIENCIACTIVA- CONCYTEC (Res. Dir. 016–2018-FONDECYT-DE; No Reg. 56747). / Producto elaborado en el marco del Proyecto de investigación dentro del Programa YACHAYNINCHIS WIÑARINANPAQ de la UNSA...
| Autores: | , , , , , |
|---|---|
| Formato: | artículo |
| Fecha de Publicación: | 2021 |
| Institución: | Consejo Nacional de Ciencia Tecnología e Innovación |
| Repositorio: | CONCYTEC-Institucional |
| Lenguaje: | inglés |
| OAI Identifier: | oai:repositorio.concytec.gob.pe:20.500.12390/3215 |
| Enlace del recurso: | https://hdl.handle.net/20.500.12390/3215 https://doi.org/10.1186/s40494-021-00619-9 |
| Nivel de acceso: | acceso abierto |
| Materia: | Nondestructive characterization Elemental analysis Iron gall ink http://purl.org/pe-repo/ocde/ford#1.05.04 |
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XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| title |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| spellingShingle |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 Luízar Obregón, Celina Nondestructive characterization Elemental analysis Elemental analysis Iron gall ink Iron gall ink http://purl.org/pe-repo/ocde/ford#1.05.04 |
| title_short |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| title_full |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| title_fullStr |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| title_full_unstemmed |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| title_sort |
XRF elemental analysis of inks in South American manuscripts from 1779 to 1825 |
| author |
Luízar Obregón, Celina |
| author_facet |
Luízar Obregón, Celina Zamalloa Jara, Marco A. Rojas Arizapana, Flor L. Chura Huayllani, Yuri J. Gonzales Bellido, Janet F. Olivera Olivera, Jorge |
| author_role |
author |
| author2 |
Zamalloa Jara, Marco A. Rojas Arizapana, Flor L. Chura Huayllani, Yuri J. Gonzales Bellido, Janet F. Olivera Olivera, Jorge |
| author2_role |
author author author author author |
| dc.contributor.author.fl_str_mv |
Luízar Obregón, Celina Zamalloa Jara, Marco A. Rojas Arizapana, Flor L. Chura Huayllani, Yuri J. Gonzales Bellido, Janet F. Olivera Olivera, Jorge |
| dc.subject.none.fl_str_mv |
Nondestructive characterization |
| topic |
Nondestructive characterization Elemental analysis Elemental analysis Iron gall ink Iron gall ink http://purl.org/pe-repo/ocde/ford#1.05.04 |
| dc.subject.es_PE.fl_str_mv |
Elemental analysis Elemental analysis Iron gall ink Iron gall ink |
| dc.subject.ocde.none.fl_str_mv |
http://purl.org/pe-repo/ocde/ford#1.05.04 |
| description |
This work was carried out with resources from the gas canon of the Cusco Region and the support of FONDECYT—CIENCIACTIVA- CONCYTEC (Res. Dir. 016–2018-FONDECYT-DE; No Reg. 56747). / Producto elaborado en el marco del Proyecto de investigación dentro del Programa YACHAYNINCHIS WIÑARINANPAQ de la UNSAAC y CONCYTEC (FONDECYT/PROCIENCIA). |
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2021 |
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2024-05-30T23:13:38Z |
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2024-05-30T23:13:38Z |
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2021-11 |
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info:eu-repo/semantics/article |
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article |
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https://hdl.handle.net/20.500.12390/3215 |
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https://doi.org/10.1186/s40494-021-00619-9 |
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2-s2.0-85118708099 |
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https://hdl.handle.net/20.500.12390/3215 https://doi.org/10.1186/s40494-021-00619-9 |
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2-s2.0-85118708099 |
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eng |
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eng |
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Heritage Science |
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info:eu-repo/semantics/openAccess |
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https://creativecommons.org/licenses/by-nc-nd/4.0/ |
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openAccess |
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https://creativecommons.org/licenses/by-nc-nd/4.0/ |
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Springer Nature |
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Springer Nature |
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CONCYTEC-Institucional |
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Publicationrp09131600rp09126600rp09127600rp09128600rp09129600rp09130600Luízar Obregón, CelinaZamalloa Jara, Marco A.Rojas Arizapana, Flor L.Chura Huayllani, Yuri J.Gonzales Bellido, Janet F.Olivera Olivera, Jorge2024-05-30T23:13:38Z2024-05-30T23:13:38Z2021-11https://hdl.handle.net/20.500.12390/3215https://doi.org/10.1186/s40494-021-00619-92-s2.0-85118708099This work was carried out with resources from the gas canon of the Cusco Region and the support of FONDECYT—CIENCIACTIVA- CONCYTEC (Res. Dir. 016–2018-FONDECYT-DE; No Reg. 56747). / Producto elaborado en el marco del Proyecto de investigación dentro del Programa YACHAYNINCHIS WIÑARINANPAQ de la UNSAAC y CONCYTEC (FONDECYT/PROCIENCIA).The Regional Archive of Cusco in Peru guards valuable history collections with exceptional regional and international value dating from the sixteenth century to the present. Historical manuscripts are part of the identity of all people; they constitute a tangible cultural heritage that must be studied, valued, and protected. In this sense, the objective of this research was to identify the chemical compositions of inks and paper, with the goals of setting the background of their originality, identifying relationships between them, and glimpsing antecedents that generated degradation due to the compositions of the inks. This study is the first of its kind in Peru and reveals the chemical elements present in the writing ink, the seal, and the paper of five documents from the late eighteenth and early nineteenth centuries. Duplicate in situ nondestructive analyses were carried out using a hand-held X-ray fluorescence spectrometer under ambient conditions in soil mode, configured with three sequential shots, and energies from zero to 40, 40, and 15 keV, respectively. The elements S and Fe were present as components of iron gall inks. Cu and Zn were less abundant; probably, they provided less corrosion and more color intensity to the inks. The minor elements Pb, As, and especially Ag in all manuscripts differentiate them from European inks of the same period. Additionally, the five documents reflect the same elemental compositions but with different concentrations. This could mean that writers used local raw materials and Spanish ink recipes. Finally, the analyses of standard reference material, SRM 1646a and SRM 196b, gave results with acceptable precision.Consejo Nacional de Ciencia, Tecnología e Innovación Tecnológica - ConcytecengSpringer NatureHeritage Scienceinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/4.0/Nondestructive characterizationElemental analysis-1Elemental analysis-1Iron gall ink-1Iron gall ink-1http://purl.org/pe-repo/ocde/ford#1.05.04-1XRF elemental analysis of inks in South American manuscripts from 1779 to 1825info:eu-repo/semantics/articlereponame:CONCYTEC-Institucionalinstname:Consejo Nacional de Ciencia Tecnología e Innovacióninstacron:CONCYTECORIGINALXRF elemental analysis of inks in South American manuscripts.pdfXRF elemental analysis of inks in South American manuscripts.pdfapplication/pdf3717515https://repositorio.concytec.gob.pe/bitstreams/9ab8a617-c30a-4c73-5acb-cef08de5b5f3/download7c2f2c1776312150c28d90d7bbadb8f6MD51THUMBNAILXRF elemental analysis of inks in South American manuscripts.pdf.jpgXRF elemental analysis of inks in South American manuscripts.pdf.jpgIM Thumbnailimage/jpeg11098https://repositorio.concytec.gob.pe/bitstreams/6c9e9864-1641-ce4b-4bb2-2f19166e54e7/download8dda2ec61241c5d37b320ba91609167aMD52TEXTXRF elemental analysis of inks in South American manuscripts.pdf.txtXRF elemental analysis of inks in South American manuscripts.pdf.txtExtracted texttext/plain48818https://repositorio.concytec.gob.pe/bitstreams/97829714-53c4-4ad0-9ddf-58310ac89be5/download14460b14ccf66197f522f56a4e134354MD5320.500.12390/3215oai:repositorio.concytec.gob.pe:20.500.12390/32152024-06-19 21:05:03.693https://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2info:eu-repo/semantics/openAccessopen accesshttps://repositorio.concytec.gob.peRepositorio Institucional CONCYTECrepositorio@concytec.gob.pe#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#<Publication xmlns="https://www.openaire.eu/cerif-profile/1.1/" id="ae5f7818-cd61-4f31-97cd-acd376538236"> <Type xmlns="https://www.openaire.eu/cerif-profile/vocab/COAR_Publication_Types">http://purl.org/coar/resource_type/c_1843</Type> <Language>eng</Language> <Title>XRF elemental analysis of inks in South American manuscripts from 1779 to 1825</Title> <PublishedIn> <Publication> <Title>Heritage Science</Title> </Publication> </PublishedIn> <PublicationDate>2021-11</PublicationDate> <DOI>https://doi.org/10.1186/s40494-021-00619-9</DOI> <SCP-Number>2-s2.0-85118708099</SCP-Number> <Authors> <Author> <DisplayName>Luízar Obregón, Celina</DisplayName> <Person id="rp09131" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Zamalloa Jara, Marco A.</DisplayName> <Person id="rp09126" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Rojas Arizapana, Flor L.</DisplayName> <Person id="rp09127" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Chura Huayllani, Yuri J.</DisplayName> <Person id="rp09128" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Gonzales Bellido, Janet F.</DisplayName> <Person id="rp09129" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Olivera Olivera, Jorge</DisplayName> <Person id="rp09130" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> </Authors> <Editors> </Editors> <Publishers> <Publisher> <DisplayName>Springer Nature</DisplayName> <OrgUnit /> </Publisher> </Publishers> <License>https://creativecommons.org/licenses/by-nc-nd/4.0/</License> <Keyword>Nondestructive characterization</Keyword> <Keyword>Elemental analysis</Keyword> <Keyword>Elemental analysis</Keyword> <Keyword>Iron gall ink</Keyword> <Keyword>Iron gall ink</Keyword> <Abstract>The Regional Archive of Cusco in Peru guards valuable history collections with exceptional regional and international value dating from the sixteenth century to the present. Historical manuscripts are part of the identity of all people; they constitute a tangible cultural heritage that must be studied, valued, and protected. In this sense, the objective of this research was to identify the chemical compositions of inks and paper, with the goals of setting the background of their originality, identifying relationships between them, and glimpsing antecedents that generated degradation due to the compositions of the inks. This study is the first of its kind in Peru and reveals the chemical elements present in the writing ink, the seal, and the paper of five documents from the late eighteenth and early nineteenth centuries. Duplicate in situ nondestructive analyses were carried out using a hand-held X-ray fluorescence spectrometer under ambient conditions in soil mode, configured with three sequential shots, and energies from zero to 40, 40, and 15 keV, respectively. The elements S and Fe were present as components of iron gall inks. Cu and Zn were less abundant; probably, they provided less corrosion and more color intensity to the inks. The minor elements Pb, As, and especially Ag in all manuscripts differentiate them from European inks of the same period. Additionally, the five documents reflect the same elemental compositions but with different concentrations. This could mean that writers used local raw materials and Spanish ink recipes. Finally, the analyses of standard reference material, SRM 1646a and SRM 196b, gave results with acceptable precision.</Abstract> <Access xmlns="http://purl.org/coar/access_right" > </Access> </Publication> -1 |
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Nota importante:
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
