The present study has as main objecuve the search of new materials, among them the porous materials whose diversity of pore diameter confers lO the same specific properties, those that in turn determine a series of applications like adsorbents. catalysts, and shield materials, among others. The investigatíon consists of the synthes1s of macroporous materials by the method Sol-Gel, using reactive of low cost as sodium silicate (silicon source) and includes/understanos the following stages: 1) control of hydrolysis of the inorganic precursors: 2) formatíon oí the rnacrostructure material (hydrothermal synthesis) and 3) elimination of the organic matter by calcinations. The structural characterization and the degree of crystalinidad were made by means of Diffraction of Rays-X (DRX) and Electronic Diffraction of Area Selecta.(DEAS), whereas the morphologic analysis was made through an Ele...

The present study has as main objecuve the search of new materials, among them the porous materials whose diversity of pore diameter confers lO the same specific properties, those that in turn determine a series of applications like adsorbents. catalysts, and shield materials, among others. The investigatíon consists of the synthes1s of macroporous materials by the method Sol-Gel, using reactive of low cost as sodium silicate (silicon source) and includes/understanos the following stages: 1) control of hydrolysis of the inorganic precursors: 2) formatíon oí the rnacrostructure material (hydrothermal synthesis) and 3) elimination of the organic matter by calcinations. The structural characterization and the degree of crystalinidad were made by means of Diffraction of Rays-X (DRX) and Electronic Diffraction of Area Selecta.(DEAS), whereas the morphologic analysis was made through an Ele...

On the base of the ceramic superconductor YBa2Cu307 obtained by SOL-GEL process whose critic temperature reached was 92 K. A new doped structure has been synthesized with calcium, in which the Ytrio has been replaced by the calcium in stoichiometry proportion Y:Ca = 0,8: 0,2 . The precursors obtained with the help of oxalate stoichiometry have been modified with calcium nitrate. The obtained matrize was treated thermally 860 ºC and 880 ºC. The characterization has been carrie through the technique of X Rays Diffraction obtained showed that the obtained materials present a high crystalline grade and a good correspondence in their crystalline structures corresponding to each superconductivity phase.

On the base of the ceramic superconductor YBa2Cu307 obtained by SOL-GEL process whose critic temperature reached was 92 K. A new doped structure has been synthesized with calcium, in which the Ytrio has been replaced by the calcium in stoichiometry proportion Y:Ca = 0,8: 0,2 . The precursors obtained with the help of oxalate stoichiometry have been modified with calcium nitrate. The obtained matrize was treated thermally 860 ºC and 880 ºC. The characterization has been carrie through the technique of X Rays Diffraction obtained showed that the obtained materials present a high crystalline grade and a good correspondence in their crystalline structures corresponding to each superconductivity phase.