SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY
Descripción del Articulo
In this work the result of the synthesis of the 4- hexil-dithiocarboxilate-1-phenil-3-methyl-2-pirazolin-5-ona(PirC6), and 4-dithiocarboxilate of dodecil-1-phenil-3-methyl-2-pirazolin-5-ona(PirC12), is presented and the products are characterized, using the microanalysis ,the infrared spectroscopy,...
| Autores: | , |
|---|---|
| Formato: | artículo |
| Fecha de Publicación: | 2015 |
| Institución: | Sociedad Química del Perú |
| Repositorio: | Revista de la Sociedad Química del Perú |
| Lenguaje: | español |
| OAI Identifier: | oai:rsqp.revistas.sqperu.org.pe:article/7 |
| Enlace del recurso: | http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/7 |
| Nivel de acceso: | acceso abierto |
| Materia: | Pyrazoline derivatives 1D and 2D NMR spectroscopy Derivados de la pirazolona espectroscopía RMN 1D y 2D |
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SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITYSÍNTESIS Y CARACTERIZACIÓN RMN 1D Y 2D DE DERIVADOS SULFURADOS DE LA 1- FENIL-3- METIL-2-PIRAZOLÍN-5-ONA Y SU POTENCIAL CAPACIDAD LIGANTEZamorano, SergioCamus, JuanPyrazoline derivatives1D and 2D NMR spectroscopyDerivados de la pirazolonaespectroscopía RMN 1D y 2DIn this work the result of the synthesis of the 4- hexil-dithiocarboxilate-1-phenil-3-methyl-2-pirazolin-5-ona(PirC6), and 4-dithiocarboxilate of dodecil-1-phenil-3-methyl-2-pirazolin-5-ona(PirC12), is presented and the products are characterized, using the microanalysis ,the infrared spectroscopy, the spectroscopy of NMR of H1 and C13 and the NMR in twodimensions (HSQC and HMBC), in order to determine their structures. In addition, theligand potential capacity of these products are studied in order to produce coordinationcompounds with the uranil (UO22+).En este trabajo se presenta el resultado de la síntesis del 4-ditiocarboxilato de hexil-1-fenil-3-metil-2-pirazolin-5-ona (PirC6) y del 4-ditiocarboxilato de dodecil-1-fenil-3-metil-2-pirazolin-5-ona (PirC12). Se caracterizan los productos obtenidos usando el microanálisis, laespectroscopía infrarroja, la espectroscopía RMN de H1 y C13 y la RMN en dos dimensiones(HSQC y HMBC) para determinar sus estructuras. Se estudia su potencial capacidad liganteen la formación de compuestos de coordinación con el UO22+.Sociedad Química del Perú2015-03-31info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttp://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/710.37761/rsqp.v81i1.7Revista de la Sociedad Química del Perú; Vol. 81 Núm. 1 (2015): Revista de la Sociedad Química del Perú; 24 - 32Journal of the Chemical Society of Peru; Vol. 81 No. 1 (2015): Journal of the Chemical Society of Peru; 24 - 322309-87401810-634X10.37761/rsqp.v81i1reponame:Revista de la Sociedad Química del Perúinstname:Sociedad Química del Perúinstacron:SQPspahttp://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/7/4Derechos de autor 2015 Sociedad Química del Perúhttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessoai:rsqp.revistas.sqperu.org.pe:article/72020-03-04T04:24:59Z |
| dc.title.none.fl_str_mv |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY SÍNTESIS Y CARACTERIZACIÓN RMN 1D Y 2D DE DERIVADOS SULFURADOS DE LA 1- FENIL-3- METIL-2-PIRAZOLÍN-5-ONA Y SU POTENCIAL CAPACIDAD LIGANTE |
| title |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| spellingShingle |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY Zamorano, Sergio Pyrazoline derivatives 1D and 2D NMR spectroscopy Derivados de la pirazolona espectroscopía RMN 1D y 2D |
| title_short |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| title_full |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| title_fullStr |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| title_full_unstemmed |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| title_sort |
SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY |
| dc.creator.none.fl_str_mv |
Zamorano, Sergio Camus, Juan |
| author |
Zamorano, Sergio |
| author_facet |
Zamorano, Sergio Camus, Juan |
| author_role |
author |
| author2 |
Camus, Juan |
| author2_role |
author |
| dc.subject.none.fl_str_mv |
Pyrazoline derivatives 1D and 2D NMR spectroscopy Derivados de la pirazolona espectroscopía RMN 1D y 2D |
| topic |
Pyrazoline derivatives 1D and 2D NMR spectroscopy Derivados de la pirazolona espectroscopía RMN 1D y 2D |
| description |
In this work the result of the synthesis of the 4- hexil-dithiocarboxilate-1-phenil-3-methyl-2-pirazolin-5-ona(PirC6), and 4-dithiocarboxilate of dodecil-1-phenil-3-methyl-2-pirazolin-5-ona(PirC12), is presented and the products are characterized, using the microanalysis ,the infrared spectroscopy, the spectroscopy of NMR of H1 and C13 and the NMR in twodimensions (HSQC and HMBC), in order to determine their structures. In addition, theligand potential capacity of these products are studied in order to produce coordinationcompounds with the uranil (UO22+). |
| publishDate |
2015 |
| dc.date.none.fl_str_mv |
2015-03-31 |
| dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
| format |
article |
| status_str |
publishedVersion |
| dc.identifier.none.fl_str_mv |
http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/7 10.37761/rsqp.v81i1.7 |
| url |
http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/7 |
| identifier_str_mv |
10.37761/rsqp.v81i1.7 |
| dc.language.none.fl_str_mv |
spa |
| language |
spa |
| dc.relation.none.fl_str_mv |
http://revistas.sqperu.org.pe/index.php/revistasqperu/article/view/7/4 |
| dc.rights.none.fl_str_mv |
Derechos de autor 2015 Sociedad Química del Perú https://creativecommons.org/licenses/by/4.0 info:eu-repo/semantics/openAccess |
| rights_invalid_str_mv |
Derechos de autor 2015 Sociedad Química del Perú https://creativecommons.org/licenses/by/4.0 |
| eu_rights_str_mv |
openAccess |
| dc.format.none.fl_str_mv |
application/pdf |
| dc.publisher.none.fl_str_mv |
Sociedad Química del Perú |
| publisher.none.fl_str_mv |
Sociedad Química del Perú |
| dc.source.none.fl_str_mv |
Revista de la Sociedad Química del Perú; Vol. 81 Núm. 1 (2015): Revista de la Sociedad Química del Perú; 24 - 32 Journal of the Chemical Society of Peru; Vol. 81 No. 1 (2015): Journal of the Chemical Society of Peru; 24 - 32 2309-8740 1810-634X 10.37761/rsqp.v81i1 reponame:Revista de la Sociedad Química del Perú instname:Sociedad Química del Perú instacron:SQP |
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Sociedad Química del Perú |
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SQP |
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SQP |
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Revista de la Sociedad Química del Perú |
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Revista de la Sociedad Química del Perú |
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1845972360893562880 |
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13.02468 |
Nota importante:
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
