New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR

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A LC-SPE-NMR system efficiently contributed to the isolation and identification of five new oleanane saponins from the roots of Dendrobangia boliviana Rusby along with twelve known saponins previously isolated from this plant and of 3- O-βD - glucuronopyranosylphytolaccagenic acid, a compound identi...

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Detalles Bibliográficos
Autores: Zebiri, Ilhem, Gratia, Audrey, Nuzillard, Jean Marc, Haddad, Mohamed, Cabanillas Amado, Billy, Harakat, Dominique, Voutquenne‐Nazabadioko, Laurence
Formato: artículo
Fecha de Publicación:2017
Institución:Instituto de investigaciones de la Amazonía Peruana
Repositorio:IIAP-Institucional
Lenguaje:inglés
OAI Identifier:oai:repositorio.iiap.gob.pe:20.500.12921/322
Enlace del recurso:https://doi.org/10.1002/mrc.4619
https://hdl.handle.net/20.500.12921/322
Nivel de acceso:acceso abierto
Materia:Dendrobangia boliviana
Saponinas
Ácidos grasos
Espectroscopia RMN
Amazonía
Compuestos bioactivos
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spelling Zebiri, IlhemGratia, AudreyNuzillard, Jean MarcHaddad, MohamedCabanillas Amado, BillyHarakat, DominiqueVoutquenne‐Nazabadioko, Laurence2018-06-28T15:55:04Z2018-06-28T15:55:04Z2017-117491581https://doi.org/10.1002/mrc.4619https://hdl.handle.net/20.500.12921/322Magnetic Resonance in Chemistryhttps://doi.org/10.1002/mrc.4619A LC-SPE-NMR system efficiently contributed to the isolation and identification of five new oleanane saponins from the roots of Dendrobangia boliviana Rusby along with twelve known saponins previously isolated from this plant and of 3- O-βD - glucuronopyranosylphytolaccagenic acid, a compound identified from Diploclisia glaucescens. Their structures were established on the basis of spectral data, mainly HR-ESIMS, 1H-NMR, HSQC, and ROESY, and by comparison with literature data. All but one of these oleanane saponins are glycosides of serjanic or phytolaccinic acid. The remaining one contained a new sapogenin, the 3β,24-dihydroxy-olean-12-en-28,30-dioic acid, 30-methyl ester or 24-hydroxy-serjanic acid, tentatively named dendrobangionic acid.engWileyinfo:eu-repo/semantics/articleMagnetic Resonance in Chemistry; 55(11) : 1036-1055https://onlinelibrary.wiley.com/doi/abs/10.1002/mrc.4619info:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-nd/2.5/pe/Instituto de Investigaciones de la Amazonía PeruanaRepositorio Institucional - IIAPreponame:IIAP-Institucionalinstname:Instituto de investigaciones de la Amazonía Peruanainstacron:IIAPDendrobangia bolivianaSaponinasÁcidos grasosEspectroscopia RMNAmazoníaCompuestos bioactivosNew oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMRinfo:eu-repo/semantics/articleORIGINALlicence.txtlicence.txttext/plain; charset=utf-8564https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/5/licence.txtd01e77160199194c1e849481498182e2MD55zebiri_articulo_2017.pdfzebiri_articulo_2017.pdfapplication/pdf433067https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/6/zebiri_articulo_2017.pdfa0f004af2fcb07593b22551e304a6941MD56TEXTNew oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR.pdf.txtNew oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR.pdf.txtExtracted texttext/plain34812https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/3/New%20oleanane%20saponins%20from%20the%20roots%20of%20Dendrobangia%20boliviana%20identified%20by%20LC%e2%80%90SPE%e2%80%90NMR.pdf.txtb468bbf82bde018e3f7b6de1f7e2ecb4MD53zebiri_articulo_2017.pdf.txtzebiri_articulo_2017.pdf.txtExtracted texttext/plain38813https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/13/zebiri_articulo_2017.pdf.txtf77a2de5f671cd5c456cfc180e96b79eMD513THUMBNAILNew oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR.pdf.jpgNew oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR.pdf.jpgGenerated Thumbnailimage/jpeg6471https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/4/New%20oleanane%20saponins%20from%20the%20roots%20of%20Dendrobangia%20boliviana%20identified%20by%20LC%e2%80%90SPE%e2%80%90NMR.pdf.jpgc594412371d7528cec68f2e95f717de6MD54zebiri_articulo_2017.pdf.jpgzebiri_articulo_2017.pdf.jpgGenerated Thumbnailimage/jpeg4408https://repositorio.iiap.gob.pe/bitstream/20.500.12921/322/14/zebiri_articulo_2017.pdf.jpgf6ef88421dedd228858a9df20adbe704MD51420.500.12921/322oai:repositorio.iiap.gob.pe:20.500.12921/3222022-12-29 19:04:58.411Repositorio Institucional del IIAPrepositorioIIAP-help@iiap.gob.pe
dc.title.es_ES.fl_str_mv New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
title New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
spellingShingle New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
Zebiri, Ilhem
Dendrobangia boliviana
Saponinas
Ácidos grasos
Espectroscopia RMN
Amazonía
Compuestos bioactivos
title_short New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
title_full New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
title_fullStr New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
title_full_unstemmed New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
title_sort New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
author Zebiri, Ilhem
author_facet Zebiri, Ilhem
Gratia, Audrey
Nuzillard, Jean Marc
Haddad, Mohamed
Cabanillas Amado, Billy
Harakat, Dominique
Voutquenne‐Nazabadioko, Laurence
author_role author
author2 Gratia, Audrey
Nuzillard, Jean Marc
Haddad, Mohamed
Cabanillas Amado, Billy
Harakat, Dominique
Voutquenne‐Nazabadioko, Laurence
author2_role author
author
author
author
author
author
dc.contributor.author.fl_str_mv Zebiri, Ilhem
Gratia, Audrey
Nuzillard, Jean Marc
Haddad, Mohamed
Cabanillas Amado, Billy
Harakat, Dominique
Voutquenne‐Nazabadioko, Laurence
dc.subject.es_ES.fl_str_mv Dendrobangia boliviana
Saponinas
Ácidos grasos
Espectroscopia RMN
Amazonía
Compuestos bioactivos
topic Dendrobangia boliviana
Saponinas
Ácidos grasos
Espectroscopia RMN
Amazonía
Compuestos bioactivos
description A LC-SPE-NMR system efficiently contributed to the isolation and identification of five new oleanane saponins from the roots of Dendrobangia boliviana Rusby along with twelve known saponins previously isolated from this plant and of 3- O-βD - glucuronopyranosylphytolaccagenic acid, a compound identified from Diploclisia glaucescens. Their structures were established on the basis of spectral data, mainly HR-ESIMS, 1H-NMR, HSQC, and ROESY, and by comparison with literature data. All but one of these oleanane saponins are glycosides of serjanic or phytolaccinic acid. The remaining one contained a new sapogenin, the 3β,24-dihydroxy-olean-12-en-28,30-dioic acid, 30-methyl ester or 24-hydroxy-serjanic acid, tentatively named dendrobangionic acid.
publishDate 2017
dc.date.accessioned.none.fl_str_mv 2018-06-28T15:55:04Z
dc.date.available.none.fl_str_mv 2018-06-28T15:55:04Z
dc.date.issued.fl_str_mv 2017-11
dc.type.es_ES.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.issn.none.fl_str_mv 7491581
dc.identifier.uri.none.fl_str_mv https://doi.org/10.1002/mrc.4619
https://hdl.handle.net/20.500.12921/322
dc.identifier.journal.es_ES.fl_str_mv Magnetic Resonance in Chemistry
dc.identifier.doi.es_ES.fl_str_mv https://doi.org/10.1002/mrc.4619
identifier_str_mv 7491581
Magnetic Resonance in Chemistry
url https://doi.org/10.1002/mrc.4619
https://hdl.handle.net/20.500.12921/322
dc.language.iso.es_ES.fl_str_mv eng
language eng
dc.relation.es_ES.fl_str_mv info:eu-repo/semantics/article
dc.relation.ispartofseries.en.fl_str_mv Magnetic Resonance in Chemistry; 55(11) : 1036-1055
dc.relation.uri.es_ES.fl_str_mv https://onlinelibrary.wiley.com/doi/abs/10.1002/mrc.4619
dc.rights.es_ES.fl_str_mv info:eu-repo/semantics/openAccess
dc.rights.uri.es_ES.fl_str_mv http://creativecommons.org/licenses/by-nc-nd/2.5/pe/
eu_rights_str_mv openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nc-nd/2.5/pe/
dc.publisher.es_ES.fl_str_mv Wiley
dc.source.es_ES.fl_str_mv Instituto de Investigaciones de la Amazonía Peruana
Repositorio Institucional - IIAP
dc.source.none.fl_str_mv reponame:IIAP-Institucional
instname:Instituto de investigaciones de la Amazonía Peruana
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instname_str Instituto de investigaciones de la Amazonía Peruana
instacron_str IIAP
institution IIAP
reponame_str IIAP-Institucional
collection IIAP-Institucional
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New oleanane saponins from the roots of Dendrobangia boliviana identified by LC‐SPE‐NMR
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