Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions
Descripción del Articulo
The authors are grateful to the former LMU students Tamara Maletin and Viviane Cocivera for their valuable contributions in the preliminary experiments to this study, to Stefanie Hoser for surface polishing of the samples and to SoHyun Park for her assistance in Rietveld refinement. This work has be...
| Autores: | , , , |
|---|---|
| Formato: | artículo |
| Fecha de Publicación: | 2017 |
| Institución: | Consejo Nacional de Ciencia Tecnología e Innovación |
| Repositorio: | CONCYTEC-Institucional |
| Lenguaje: | inglés |
| OAI Identifier: | oai:repositorio.concytec.gob.pe:20.500.12390/1197 |
| Enlace del recurso: | https://hdl.handle.net/20.500.12390/1197 https://doi.org/10.1016/j.jcrysgro.2017.07.016 |
| Nivel de acceso: | acceso abierto |
| Materia: | Thermoelectrics A1. Phase diagramsA2 Bridgman methodA2 Growth from high-temperature solutionsB1 Intermetallic compoundsB2 https://purl.org/pe-repo/ocde/ford#1.04.00 |
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4689 |
| dc.title.none.fl_str_mv |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| title |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| spellingShingle |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions Pillaca, M Thermoelectrics A1. Phase diagramsA2 Bridgman methodA2 Growth from high-temperature solutionsB1 Intermetallic compoundsB2 https://purl.org/pe-repo/ocde/ford#1.04.00 |
| title_short |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| title_full |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| title_fullStr |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| title_full_unstemmed |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| title_sort |
Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions |
| author |
Pillaca, M |
| author_facet |
Pillaca, M Harder, O Miller, W Gille, P |
| author_role |
author |
| author2 |
Harder, O Miller, W Gille, P |
| author2_role |
author author author |
| dc.contributor.author.fl_str_mv |
Pillaca, M Harder, O Miller, W Gille, P |
| dc.subject.none.fl_str_mv |
Thermoelectrics |
| topic |
Thermoelectrics A1. Phase diagramsA2 Bridgman methodA2 Growth from high-temperature solutionsB1 Intermetallic compoundsB2 https://purl.org/pe-repo/ocde/ford#1.04.00 |
| dc.subject.es_PE.fl_str_mv |
A1. Phase diagramsA2 Bridgman methodA2 Growth from high-temperature solutionsB1 Intermetallic compoundsB2 |
| dc.subject.ocde.none.fl_str_mv |
https://purl.org/pe-repo/ocde/ford#1.04.00 |
| description |
The authors are grateful to the former LMU students Tamara Maletin and Viviane Cocivera for their valuable contributions in the preliminary experiments to this study, to Stefanie Hoser for surface polishing of the samples and to SoHyun Park for her assistance in Rietveld refinement. This work has been partly conducted within the European integrated Center for the development of new Metallic Alloys and Compounds. M.P. is grateful for funding by the Peruvian Council of Science and Technology (CONCYTEC), grant no. 221-2014-FONDECYT. |
| publishDate |
2017 |
| dc.date.accessioned.none.fl_str_mv |
2024-05-30T23:13:38Z |
| dc.date.available.none.fl_str_mv |
2024-05-30T23:13:38Z |
| dc.date.issued.fl_str_mv |
2017 |
| dc.type.none.fl_str_mv |
info:eu-repo/semantics/article |
| format |
article |
| dc.identifier.uri.none.fl_str_mv |
https://hdl.handle.net/20.500.12390/1197 |
| dc.identifier.doi.none.fl_str_mv |
https://doi.org/10.1016/j.jcrysgro.2017.07.016 |
| dc.identifier.isi.none.fl_str_mv |
410916300051 |
| url |
https://hdl.handle.net/20.500.12390/1197 https://doi.org/10.1016/j.jcrysgro.2017.07.016 |
| identifier_str_mv |
410916300051 |
| dc.language.iso.none.fl_str_mv |
eng |
| language |
eng |
| dc.relation.ispartof.none.fl_str_mv |
Journal of Crystal Growth |
| dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess |
| eu_rights_str_mv |
openAccess |
| dc.publisher.none.fl_str_mv |
Elsevier B.V. |
| publisher.none.fl_str_mv |
Elsevier B.V. |
| dc.source.none.fl_str_mv |
reponame:CONCYTEC-Institucional instname:Consejo Nacional de Ciencia Tecnología e Innovación instacron:CONCYTEC |
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Consejo Nacional de Ciencia Tecnología e Innovación |
| instacron_str |
CONCYTEC |
| institution |
CONCYTEC |
| reponame_str |
CONCYTEC-Institucional |
| collection |
CONCYTEC-Institucional |
| repository.name.fl_str_mv |
Repositorio Institucional CONCYTEC |
| repository.mail.fl_str_mv |
repositorio@concytec.gob.pe |
| _version_ |
1844883020917506048 |
| spelling |
Publicationrp03417600rp03418600rp01673500rp03419600Pillaca, MHarder, OMiller, WGille, P2024-05-30T23:13:38Z2024-05-30T23:13:38Z2017https://hdl.handle.net/20.500.12390/1197https://doi.org/10.1016/j.jcrysgro.2017.07.016410916300051The authors are grateful to the former LMU students Tamara Maletin and Viviane Cocivera for their valuable contributions in the preliminary experiments to this study, to Stefanie Hoser for surface polishing of the samples and to SoHyun Park for her assistance in Rietveld refinement. This work has been partly conducted within the European integrated Center for the development of new Metallic Alloys and Compounds. M.P. is grateful for funding by the Peruvian Council of Science and Technology (CONCYTEC), grant no. 221-2014-FONDECYT.Sb-based compounds such as CoSb3 and FeSb2 are interesting materials for thermoelectric applications. Their single crystal growth can be achieved from high-temperature solutions that are strongly enriched in Sb. In Bridgman growth using closed ampoules, effective mixing of the solution is an important prerequisite in order to minimize the high risk of liquid inclusion formation. We have successfully grown inclusion-free single crystal of CoSb3 and FeSb2 by rotating the ampoule in a Bridgman-type crystal growth set-up being inclined by 75° with respect to the vector of gravity. Numerical modelling as well as experimental growth studies have demonstrated the strong influence of forced convection that is achieved by this modified directional solidification technique called Inclined Rotary Bridgman method.Consejo Nacional de Ciencia, Tecnología e Innovación Tecnológica - ConcytecengElsevier B.V.Journal of Crystal Growthinfo:eu-repo/semantics/openAccessThermoelectricsA1. Phase diagramsA2-1Bridgman methodA2-1Growth from high-temperature solutionsB1-1Intermetallic compoundsB2-1https://purl.org/pe-repo/ocde/ford#1.04.00-1Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutionsinfo:eu-repo/semantics/articlereponame:CONCYTEC-Institucionalinstname:Consejo Nacional de Ciencia Tecnología e Innovacióninstacron:CONCYTEC#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#20.500.12390/1197oai:repositorio.concytec.gob.pe:20.500.12390/11972024-05-30 15:23:53.459http://purl.org/coar/access_right/c_14cbinfo:eu-repo/semantics/closedAccessmetadata only accesshttps://repositorio.concytec.gob.peRepositorio Institucional CONCYTECrepositorio@concytec.gob.pe#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#<Publication xmlns="https://www.openaire.eu/cerif-profile/1.1/" id="b8ab18b1-9612-4ed6-86da-90a850a743ea"> <Type xmlns="https://www.openaire.eu/cerif-profile/vocab/COAR_Publication_Types">http://purl.org/coar/resource_type/c_1843</Type> <Language>eng</Language> <Title>Forced convection by Inclined Rotary Bridgman method for growth of CoSb3 and FeSb2 single crystals from Sb-rich solutions</Title> <PublishedIn> <Publication> <Title>Journal of Crystal Growth</Title> </Publication> </PublishedIn> <PublicationDate>2017</PublicationDate> <DOI>https://doi.org/10.1016/j.jcrysgro.2017.07.016</DOI> <ISI-Number>410916300051</ISI-Number> <Authors> <Author> <DisplayName>Pillaca, M</DisplayName> <Person id="rp03417" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Harder, O</DisplayName> <Person id="rp03418" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Miller, W</DisplayName> <Person id="rp01673" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Gille, P</DisplayName> <Person id="rp03419" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> </Authors> <Editors> </Editors> <Publishers> <Publisher> <DisplayName>Elsevier B.V.</DisplayName> <OrgUnit /> </Publisher> </Publishers> <Keyword>Thermoelectrics</Keyword> <Keyword>A1. Phase diagramsA2</Keyword> <Keyword>Bridgman methodA2</Keyword> <Keyword>Growth from high-temperature solutionsB1</Keyword> <Keyword>Intermetallic compoundsB2</Keyword> <Abstract>Sb-based compounds such as CoSb3 and FeSb2 are interesting materials for thermoelectric applications. Their single crystal growth can be achieved from high-temperature solutions that are strongly enriched in Sb. In Bridgman growth using closed ampoules, effective mixing of the solution is an important prerequisite in order to minimize the high risk of liquid inclusion formation. We have successfully grown inclusion-free single crystal of CoSb3 and FeSb2 by rotating the ampoule in a Bridgman-type crystal growth set-up being inclined by 75° with respect to the vector of gravity. Numerical modelling as well as experimental growth studies have demonstrated the strong influence of forced convection that is achieved by this modified directional solidification technique called Inclined Rotary Bridgman method.</Abstract> <Access xmlns="http://purl.org/coar/access_right" > </Access> </Publication> -1 |
| score |
13.394457 |
Nota importante:
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
