Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
Descripción del Articulo
Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM I...
Autores: | , , , |
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Formato: | artículo |
Fecha de Publicación: | 2022 |
Institución: | Consejo Nacional de Ciencia Tecnología e Innovación |
Repositorio: | CONCYTEC-Institucional |
Lenguaje: | inglés |
OAI Identifier: | oai:repositorio.concytec.gob.pe:20.500.12390/3008 |
Enlace del recurso: | https://hdl.handle.net/20.500.12390/3008 https://doi.org/10.32604/jrm.2022.017377 |
Nivel de acceso: | acceso abierto |
Materia: | ZnO nanoparticles Green chemistry Moringa oleifera extract Optical characterization Structural characterization https://purl.org/pe-repo/ocde/ford#2.10.02 |
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4689 |
dc.title.none.fl_str_mv |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
title |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
spellingShingle |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera González-Fernández J.V. ZnO nanoparticles Green chemistry Green chemistry Moringa oleifera extract Moringa oleifera extract Optical characterization Structural characterization https://purl.org/pe-repo/ocde/ford#2.10.02 |
title_short |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
title_full |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
title_fullStr |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
title_full_unstemmed |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
title_sort |
Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera |
author |
González-Fernández J.V. |
author_facet |
González-Fernández J.V. Pinzón-Moreno D.D. Neciosup-Puican A.A. Carranza-Oropeza M.V. |
author_role |
author |
author2 |
Pinzón-Moreno D.D. Neciosup-Puican A.A. Carranza-Oropeza M.V. |
author2_role |
author author author |
dc.contributor.author.fl_str_mv |
González-Fernández J.V. Pinzón-Moreno D.D. Neciosup-Puican A.A. Carranza-Oropeza M.V. |
dc.subject.none.fl_str_mv |
ZnO nanoparticles |
topic |
ZnO nanoparticles Green chemistry Green chemistry Moringa oleifera extract Moringa oleifera extract Optical characterization Structural characterization https://purl.org/pe-repo/ocde/ford#2.10.02 |
dc.subject.es_PE.fl_str_mv |
Green chemistry Green chemistry Moringa oleifera extract Moringa oleifera extract Optical characterization Structural characterization |
dc.subject.ocde.none.fl_str_mv |
https://purl.org/pe-repo/ocde/ford#2.10.02 |
description |
Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM INC.INV. |
publishDate |
2022 |
dc.date.accessioned.none.fl_str_mv |
2024-05-30T23:13:38Z |
dc.date.available.none.fl_str_mv |
2024-05-30T23:13:38Z |
dc.date.issued.fl_str_mv |
2022 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
dc.identifier.uri.none.fl_str_mv |
https://hdl.handle.net/20.500.12390/3008 |
dc.identifier.doi.none.fl_str_mv |
https://doi.org/10.32604/jrm.2022.017377 |
dc.identifier.scopus.none.fl_str_mv |
2-s2.0-85116430539 |
url |
https://hdl.handle.net/20.500.12390/3008 https://doi.org/10.32604/jrm.2022.017377 |
identifier_str_mv |
2-s2.0-85116430539 |
dc.language.iso.none.fl_str_mv |
eng |
language |
eng |
dc.relation.ispartof.none.fl_str_mv |
Journal of Renewable Materials |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess |
dc.rights.uri.none.fl_str_mv |
https://creativecommons.org/licenses/by-nc-nd/4.0/ |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-nd/4.0/ |
dc.publisher.none.fl_str_mv |
Tech Science Press |
publisher.none.fl_str_mv |
Tech Science Press |
dc.source.none.fl_str_mv |
reponame:CONCYTEC-Institucional instname:Consejo Nacional de Ciencia Tecnología e Innovación instacron:CONCYTEC |
instname_str |
Consejo Nacional de Ciencia Tecnología e Innovación |
instacron_str |
CONCYTEC |
institution |
CONCYTEC |
reponame_str |
CONCYTEC-Institucional |
collection |
CONCYTEC-Institucional |
repository.name.fl_str_mv |
Repositorio Institucional CONCYTEC |
repository.mail.fl_str_mv |
repositorio@concytec.gob.pe |
_version_ |
1839175423564447744 |
spelling |
Publicationrp08598600rp08597600rp08600600rp08599600González-Fernández J.V.Pinzón-Moreno D.D.Neciosup-Puican A.A.Carranza-Oropeza M.V.2024-05-30T23:13:38Z2024-05-30T23:13:38Z2022https://hdl.handle.net/20.500.12390/3008https://doi.org/10.32604/jrm.2022.0173772-s2.0-85116430539Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM INC.INV.ZnO nanoparticles (ZnO-NP) present innovative optical, electrical, and magnetic properties that depend on spe-cific characteristics, e.g., size, distribution, and morphology. Thus, these properties are essential to address various applications in areas such as electronics, medicine, energy, and others. In addition, the performance of this ZnO-NP depends of their preparation which can be done by chemical, physical, and biological methods. Meanwhile, nowadays, the main interest in developing ZnO-NP synthesis through biological methods bases on the decrease of use of toxic chemicals or energy applied to the procedures, making the process more cost-effective and environmentally friendly. However, the large-scale production of nanoparticles by green synthesis remains a big challenge due to the complexity of the biological extracts used in chemical reactions. That being the case, the preparation of ZnO-NP using Moringa oleifera extract as an alternative biological agent for capping and reduction in synthesis was evaluated in this work. Then, the results based on the analysis of the optical and structural characterization of the ZnO-NP obtained by employing UV-Vis, DLS, zeta potential, XRD, ATR-FTIR, and FE-SEM indicate mostly the presence of spherical nanosized material with a mean hydrodynamic diameter of 47.2 nm measured by DLS and a mean size diameter of 25 nm observed with FE-SEM technique. Furthermore, in FE-SEM images a homo-geneous dispersion and distribution is observed in the absence of agglutination, agglomeration, or generation of significant lumps of the ZnO-NP. The XRD analysis showed that heat annealing induced the crystallite size favor-ing their monocrystallinity. Those obtained data confirm the synthesis of ZnO-NP and the absence of impurities associated with organic compounds in the annealed samples. Finally, those results and low-cost production present to the synthesized ZnO-NP by this biological method as a useful material in several applications. © 2022, Tech Science Press. All rights reserved.Consejo Nacional de Ciencia, Tecnología e Innovación Tecnológica - ConcytecengTech Science PressJournal of Renewable Materialsinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/4.0/ZnO nanoparticlesGreen chemistry-1Green chemistry-1Moringa oleifera extract-1Moringa oleifera extract-1Optical characterization-1Structural characterization-1https://purl.org/pe-repo/ocde/ford#2.10.02-1Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleiferainfo:eu-repo/semantics/articlereponame:CONCYTEC-Institucionalinstname:Consejo Nacional de Ciencia Tecnología e Innovacióninstacron:CONCYTEC20.500.12390/3008oai:repositorio.concytec.gob.pe:20.500.12390/30082024-05-30 16:13:05.248https://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_14cbinfo:eu-repo/semantics/closedAccessmetadata only accesshttps://repositorio.concytec.gob.peRepositorio Institucional CONCYTECrepositorio@concytec.gob.pe#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#<Publication xmlns="https://www.openaire.eu/cerif-profile/1.1/" id="13163c31-c570-429e-8bbf-e979f51d1e3f"> <Type xmlns="https://www.openaire.eu/cerif-profile/vocab/COAR_Publication_Types">http://purl.org/coar/resource_type/c_1843</Type> <Language>eng</Language> <Title>Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera</Title> <PublishedIn> <Publication> <Title>Journal of Renewable Materials</Title> </Publication> </PublishedIn> <PublicationDate>2022</PublicationDate> <DOI>https://doi.org/10.32604/jrm.2022.017377</DOI> <SCP-Number>2-s2.0-85116430539</SCP-Number> <Authors> <Author> <DisplayName>González-Fernández J.V.</DisplayName> <Person id="rp08598" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Pinzón-Moreno D.D.</DisplayName> <Person id="rp08597" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Neciosup-Puican A.A.</DisplayName> <Person id="rp08600" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Carranza-Oropeza M.V.</DisplayName> <Person id="rp08599" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> </Authors> <Editors> </Editors> <Publishers> <Publisher> <DisplayName>Tech Science Press</DisplayName> <OrgUnit /> </Publisher> </Publishers> <License>https://creativecommons.org/licenses/by-nc-nd/4.0/</License> <Keyword>ZnO nanoparticles</Keyword> <Keyword>Green chemistry</Keyword> <Keyword>Green chemistry</Keyword> <Keyword>Moringa oleifera extract</Keyword> <Keyword>Moringa oleifera extract</Keyword> <Keyword>Optical characterization</Keyword> <Keyword>Structural characterization</Keyword> <Abstract>ZnO nanoparticles (ZnO-NP) present innovative optical, electrical, and magnetic properties that depend on spe-cific characteristics, e.g., size, distribution, and morphology. Thus, these properties are essential to address various applications in areas such as electronics, medicine, energy, and others. In addition, the performance of this ZnO-NP depends of their preparation which can be done by chemical, physical, and biological methods. Meanwhile, nowadays, the main interest in developing ZnO-NP synthesis through biological methods bases on the decrease of use of toxic chemicals or energy applied to the procedures, making the process more cost-effective and environmentally friendly. However, the large-scale production of nanoparticles by green synthesis remains a big challenge due to the complexity of the biological extracts used in chemical reactions. That being the case, the preparation of ZnO-NP using Moringa oleifera extract as an alternative biological agent for capping and reduction in synthesis was evaluated in this work. Then, the results based on the analysis of the optical and structural characterization of the ZnO-NP obtained by employing UV-Vis, DLS, zeta potential, XRD, ATR-FTIR, and FE-SEM indicate mostly the presence of spherical nanosized material with a mean hydrodynamic diameter of 47.2 nm measured by DLS and a mean size diameter of 25 nm observed with FE-SEM technique. Furthermore, in FE-SEM images a homo-geneous dispersion and distribution is observed in the absence of agglutination, agglomeration, or generation of significant lumps of the ZnO-NP. The XRD analysis showed that heat annealing induced the crystallite size favor-ing their monocrystallinity. Those obtained data confirm the synthesis of ZnO-NP and the absence of impurities associated with organic compounds in the annealed samples. Finally, those results and low-cost production present to the synthesized ZnO-NP by this biological method as a useful material in several applications. © 2022, Tech Science Press. All rights reserved.</Abstract> <Access xmlns="http://purl.org/coar/access_right" > </Access> </Publication> -1 |
score |
13.439101 |
Nota importante:
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).