Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera

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Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM I...

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Autores: González-Fernández J.V., Pinzón-Moreno D.D., Neciosup-Puican A.A., Carranza-Oropeza M.V.
Formato: artículo
Fecha de Publicación:2022
Institución:Consejo Nacional de Ciencia Tecnología e Innovación
Repositorio:CONCYTEC-Institucional
Lenguaje:inglés
OAI Identifier:oai:repositorio.concytec.gob.pe:20.500.12390/3008
Enlace del recurso:https://hdl.handle.net/20.500.12390/3008
https://doi.org/10.32604/jrm.2022.017377
Nivel de acceso:acceso abierto
Materia:ZnO nanoparticles
Green chemistry
Moringa oleifera extract
Optical characterization
Structural characterization
https://purl.org/pe-repo/ocde/ford#2.10.02
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oai_identifier_str oai:repositorio.concytec.gob.pe:20.500.12390/3008
network_acronym_str CONC
network_name_str CONCYTEC-Institucional
repository_id_str 4689
dc.title.none.fl_str_mv Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
title Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
spellingShingle Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
González-Fernández J.V.
ZnO nanoparticles
Green chemistry
Green chemistry
Moringa oleifera extract
Moringa oleifera extract
Optical characterization
Structural characterization
https://purl.org/pe-repo/ocde/ford#2.10.02
title_short Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
title_full Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
title_fullStr Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
title_full_unstemmed Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
title_sort Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera
author González-Fernández J.V.
author_facet González-Fernández J.V.
Pinzón-Moreno D.D.
Neciosup-Puican A.A.
Carranza-Oropeza M.V.
author_role author
author2 Pinzón-Moreno D.D.
Neciosup-Puican A.A.
Carranza-Oropeza M.V.
author2_role author
author
author
dc.contributor.author.fl_str_mv González-Fernández J.V.
Pinzón-Moreno D.D.
Neciosup-Puican A.A.
Carranza-Oropeza M.V.
dc.subject.none.fl_str_mv ZnO nanoparticles
topic ZnO nanoparticles
Green chemistry
Green chemistry
Moringa oleifera extract
Moringa oleifera extract
Optical characterization
Structural characterization
https://purl.org/pe-repo/ocde/ford#2.10.02
dc.subject.es_PE.fl_str_mv Green chemistry
Green chemistry
Moringa oleifera extract
Moringa oleifera extract
Optical characterization
Structural characterization
dc.subject.ocde.none.fl_str_mv https://purl.org/pe-repo/ocde/ford#2.10.02
description Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM INC.INV.
publishDate 2022
dc.date.accessioned.none.fl_str_mv 2024-05-30T23:13:38Z
dc.date.available.none.fl_str_mv 2024-05-30T23:13:38Z
dc.date.issued.fl_str_mv 2022
dc.type.none.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.uri.none.fl_str_mv https://hdl.handle.net/20.500.12390/3008
dc.identifier.doi.none.fl_str_mv https://doi.org/10.32604/jrm.2022.017377
dc.identifier.scopus.none.fl_str_mv 2-s2.0-85116430539
url https://hdl.handle.net/20.500.12390/3008
https://doi.org/10.32604/jrm.2022.017377
identifier_str_mv 2-s2.0-85116430539
dc.language.iso.none.fl_str_mv eng
language eng
dc.relation.ispartof.none.fl_str_mv Journal of Renewable Materials
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
dc.rights.uri.none.fl_str_mv https://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/4.0/
dc.publisher.none.fl_str_mv Tech Science Press
publisher.none.fl_str_mv Tech Science Press
dc.source.none.fl_str_mv reponame:CONCYTEC-Institucional
instname:Consejo Nacional de Ciencia Tecnología e Innovación
instacron:CONCYTEC
instname_str Consejo Nacional de Ciencia Tecnología e Innovación
instacron_str CONCYTEC
institution CONCYTEC
reponame_str CONCYTEC-Institucional
collection CONCYTEC-Institucional
repository.name.fl_str_mv Repositorio Institucional CONCYTEC
repository.mail.fl_str_mv repositorio@concytec.gob.pe
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spelling Publicationrp08598600rp08597600rp08600600rp08599600González-Fernández J.V.Pinzón-Moreno D.D.Neciosup-Puican A.A.Carranza-Oropeza M.V.2024-05-30T23:13:38Z2024-05-30T23:13:38Z2022https://hdl.handle.net/20.500.12390/3008https://doi.org/10.32604/jrm.2022.0173772-s2.0-85116430539Funding Statement: Authors are grateful to Concytec-Peru and The World Bank for the financial support of this project under the call “Mejoramiento y Ampliación de los Servicios del Sistema Nacional de Ciencia Tecnología e Innovación Tecnológica” 8682-PE, through Fondecyt Grant 017-2019 FONDECYT BM INC.INV.ZnO nanoparticles (ZnO-NP) present innovative optical, electrical, and magnetic properties that depend on spe-cific characteristics, e.g., size, distribution, and morphology. Thus, these properties are essential to address various applications in areas such as electronics, medicine, energy, and others. In addition, the performance of this ZnO-NP depends of their preparation which can be done by chemical, physical, and biological methods. Meanwhile, nowadays, the main interest in developing ZnO-NP synthesis through biological methods bases on the decrease of use of toxic chemicals or energy applied to the procedures, making the process more cost-effective and environmentally friendly. However, the large-scale production of nanoparticles by green synthesis remains a big challenge due to the complexity of the biological extracts used in chemical reactions. That being the case, the preparation of ZnO-NP using Moringa oleifera extract as an alternative biological agent for capping and reduction in synthesis was evaluated in this work. Then, the results based on the analysis of the optical and structural characterization of the ZnO-NP obtained by employing UV-Vis, DLS, zeta potential, XRD, ATR-FTIR, and FE-SEM indicate mostly the presence of spherical nanosized material with a mean hydrodynamic diameter of 47.2 nm measured by DLS and a mean size diameter of 25 nm observed with FE-SEM technique. Furthermore, in FE-SEM images a homo-geneous dispersion and distribution is observed in the absence of agglutination, agglomeration, or generation of significant lumps of the ZnO-NP. The XRD analysis showed that heat annealing induced the crystallite size favor-ing their monocrystallinity. Those obtained data confirm the synthesis of ZnO-NP and the absence of impurities associated with organic compounds in the annealed samples. Finally, those results and low-cost production present to the synthesized ZnO-NP by this biological method as a useful material in several applications. © 2022, Tech Science Press. All rights reserved.Consejo Nacional de Ciencia, Tecnología e Innovación Tecnológica - ConcytecengTech Science PressJournal of Renewable Materialsinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/4.0/ZnO nanoparticlesGreen chemistry-1Green chemistry-1Moringa oleifera extract-1Moringa oleifera extract-1Optical characterization-1Structural characterization-1https://purl.org/pe-repo/ocde/ford#2.10.02-1Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleiferainfo:eu-repo/semantics/articlereponame:CONCYTEC-Institucionalinstname:Consejo Nacional de Ciencia Tecnología e Innovacióninstacron:CONCYTEC20.500.12390/3008oai:repositorio.concytec.gob.pe:20.500.12390/30082024-05-30 16:13:05.248https://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_14cbinfo:eu-repo/semantics/closedAccessmetadata only accesshttps://repositorio.concytec.gob.peRepositorio Institucional CONCYTECrepositorio@concytec.gob.pe#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#<Publication xmlns="https://www.openaire.eu/cerif-profile/1.1/" id="13163c31-c570-429e-8bbf-e979f51d1e3f"> <Type xmlns="https://www.openaire.eu/cerif-profile/vocab/COAR_Publication_Types">http://purl.org/coar/resource_type/c_1843</Type> <Language>eng</Language> <Title>Green method, optical and structural characterization of zno nanoparticles synthesized using leaves extract of m. Oleifera</Title> <PublishedIn> <Publication> <Title>Journal of Renewable Materials</Title> </Publication> </PublishedIn> <PublicationDate>2022</PublicationDate> <DOI>https://doi.org/10.32604/jrm.2022.017377</DOI> <SCP-Number>2-s2.0-85116430539</SCP-Number> <Authors> <Author> <DisplayName>González-Fernández J.V.</DisplayName> <Person id="rp08598" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Pinzón-Moreno D.D.</DisplayName> <Person id="rp08597" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Neciosup-Puican A.A.</DisplayName> <Person id="rp08600" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> <Author> <DisplayName>Carranza-Oropeza M.V.</DisplayName> <Person id="rp08599" /> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> </Authors> <Editors> </Editors> <Publishers> <Publisher> <DisplayName>Tech Science Press</DisplayName> <OrgUnit /> </Publisher> </Publishers> <License>https://creativecommons.org/licenses/by-nc-nd/4.0/</License> <Keyword>ZnO nanoparticles</Keyword> <Keyword>Green chemistry</Keyword> <Keyword>Green chemistry</Keyword> <Keyword>Moringa oleifera extract</Keyword> <Keyword>Moringa oleifera extract</Keyword> <Keyword>Optical characterization</Keyword> <Keyword>Structural characterization</Keyword> <Abstract>ZnO nanoparticles (ZnO-NP) present innovative optical, electrical, and magnetic properties that depend on spe-cific characteristics, e.g., size, distribution, and morphology. Thus, these properties are essential to address various applications in areas such as electronics, medicine, energy, and others. In addition, the performance of this ZnO-NP depends of their preparation which can be done by chemical, physical, and biological methods. Meanwhile, nowadays, the main interest in developing ZnO-NP synthesis through biological methods bases on the decrease of use of toxic chemicals or energy applied to the procedures, making the process more cost-effective and environmentally friendly. However, the large-scale production of nanoparticles by green synthesis remains a big challenge due to the complexity of the biological extracts used in chemical reactions. That being the case, the preparation of ZnO-NP using Moringa oleifera extract as an alternative biological agent for capping and reduction in synthesis was evaluated in this work. Then, the results based on the analysis of the optical and structural characterization of the ZnO-NP obtained by employing UV-Vis, DLS, zeta potential, XRD, ATR-FTIR, and FE-SEM indicate mostly the presence of spherical nanosized material with a mean hydrodynamic diameter of 47.2 nm measured by DLS and a mean size diameter of 25 nm observed with FE-SEM technique. Furthermore, in FE-SEM images a homo-geneous dispersion and distribution is observed in the absence of agglutination, agglomeration, or generation of significant lumps of the ZnO-NP. The XRD analysis showed that heat annealing induced the crystallite size favor-ing their monocrystallinity. Those obtained data confirm the synthesis of ZnO-NP and the absence of impurities associated with organic compounds in the annealed samples. Finally, those results and low-cost production present to the synthesized ZnO-NP by this biological method as a useful material in several applications. © 2022, Tech Science Press. All rights reserved.</Abstract> <Access xmlns="http://purl.org/coar/access_right" > </Access> </Publication> -1
score 13.439101
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