1
artículo
Publicado 2022
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The Soxhlet method in extracting plasticizers from PVC compounds presents various areas for improvement, such as the amount of solvent used, the time required in the process, and its costs. This study proposes replacing the Soxhlet method with the ultrasound-assisted method to reduce the time, costs, and amount of solvent used in plasticizer extraction. It also proposes using solvent recovered from previous extractions to reduce costs further. The study involved experimentation with three different grades of PVC compounds (medical, cable, and profile) to compare the recovery of plasticizers by the Soxhlet and the ultrasound-assisted methods. The plasticizers obtained were analyzed using gas chromatography, gas chromatography coupled with mass spectroscopy, and Fourier-transform infrared spectroscopy to evaluate the results of each extraction method as compared to reference co...
2
artículo
Publicado 2022
Enlace
Enlace
The Soxhlet method in extracting plasticizers from PVC compounds presents various areas for improvement, such as the amount of solvent used, the time required in the process, and its costs. This study proposes replacing the Soxhlet method with the ultrasound-assisted method to reduce the time, costs, and amount of solvent used in plasticizer extraction. It also proposes using solvent recovered from previous extractions to reduce costs further. The study involved experimentation with three different grades of PVC compounds (medical, cable, and profile) to compare the recovery of plasticizers by the Soxhlet and the ultrasound-assisted methods. The plasticizers obtained were analyzed using gas chromatography, gas chromatography coupled with mass spectroscopy, and Fourier-transform infrared spectroscopy to evaluate the results of each extraction method as compared to reference co...