Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing
Descripción del Articulo
20th LACCEI International Multi-Conference forEngineering, Education, and Technology: “Education, Research and Leadership in Post-pandemic Engineering: Resilient, Inclusive and Sustainable Actions”
| Autores: | , , , , |
|---|---|
| Formato: | objeto de conferencia |
| Fecha de Publicación: | 2022 |
| Institución: | Universidad Tecnológica del Perú |
| Repositorio: | UTP-Institucional |
| Lenguaje: | español |
| OAI Identifier: | oai:repositorio.utp.edu.pe:20.500.12867/9807 |
| Enlace del recurso: | https://hdl.handle.net/20.500.12867/9807 |
| Nivel de acceso: | acceso abierto |
| Materia: | Soils Chlorpyrifos Methamidophos Thin Layer Chromatigraphy Image Processing https://purl.org/pe-repo/ocde/ford#2.11.04 |
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Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| dc.title.alternative.es_PE.fl_str_mv |
Desarrollo de un método rápido para la cuantificación de metamidofos y clorpirifós por cromatografía en capa fina en suelos mediante procesamiento de imágenes |
| title |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| spellingShingle |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing Gonzales-Condori, Elvis Gilmar Soils Chlorpyrifos Methamidophos Thin Layer Chromatigraphy Image Processing https://purl.org/pe-repo/ocde/ford#2.11.04 |
| title_short |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| title_full |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| title_fullStr |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| title_full_unstemmed |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| title_sort |
Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processing |
| author |
Gonzales-Condori, Elvis Gilmar |
| author_facet |
Gonzales-Condori, Elvis Gilmar Reynoso-Espinoza, Juan Carlos Yucra-Condori, Ricardo Kenedy Ramirez, J. Choquenaira-Quispe, Celia |
| author_role |
author |
| author2 |
Reynoso-Espinoza, Juan Carlos Yucra-Condori, Ricardo Kenedy Ramirez, J. Choquenaira-Quispe, Celia |
| author2_role |
author author author author |
| dc.contributor.author.fl_str_mv |
Gonzales-Condori, Elvis Gilmar Reynoso-Espinoza, Juan Carlos Yucra-Condori, Ricardo Kenedy Ramirez, J. Choquenaira-Quispe, Celia |
| dc.subject.es_PE.fl_str_mv |
Soils Chlorpyrifos Methamidophos Thin Layer Chromatigraphy Image Processing |
| topic |
Soils Chlorpyrifos Methamidophos Thin Layer Chromatigraphy Image Processing https://purl.org/pe-repo/ocde/ford#2.11.04 |
| dc.subject.ocde.es_PE.fl_str_mv |
https://purl.org/pe-repo/ocde/ford#2.11.04 |
| description |
20th LACCEI International Multi-Conference forEngineering, Education, and Technology: “Education, Research and Leadership in Post-pandemic Engineering: Resilient, Inclusive and Sustainable Actions” |
| publishDate |
2022 |
| dc.date.accessioned.none.fl_str_mv |
2024-09-30T23:24:47Z |
| dc.date.available.none.fl_str_mv |
2024-09-30T23:24:47Z |
| dc.date.issued.fl_str_mv |
2022 |
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info:eu-repo/semantics/conferenceObject |
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978-628952070-5 |
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2414-6390 |
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https://hdl.handle.net/20.500.12867/9807 |
| dc.identifier.journal.es_PE.fl_str_mv |
Proceedings of the LACCEI international Multi-conference for Engineering, Education and Technology |
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10.18687/LACCEI2022.1.1.781 |
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978-628952070-5 2414-6390 Proceedings of the LACCEI international Multi-conference for Engineering, Education and Technology 10.18687/LACCEI2022.1.1.781 |
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https://hdl.handle.net/20.500.12867/9807 |
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spa |
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spa |
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Proceedings of the LACCEI international Multi-conference for Engineering, Education and Technology;Vol. 2022-July |
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info:eu-repo/semantics/openAccess |
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http://creativecommons.org/licenses/by-nc-sa/4.0/ |
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Latin American and Caribbean Consortium for Engineering Institutions |
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PE |
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Repositorio Institucional - UTP Universidad Tecnológica del Perú |
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Gonzales-Condori, Elvis GilmarReynoso-Espinoza, Juan CarlosYucra-Condori, RicardoKenedy Ramirez, J.Choquenaira-Quispe, Celia2024-09-30T23:24:47Z2024-09-30T23:24:47Z2022978-628952070-52414-6390https://hdl.handle.net/20.500.12867/9807Proceedings of the LACCEI international Multi-conference for Engineering, Education and Technology10.18687/LACCEI2022.1.1.78120th LACCEI International Multi-Conference forEngineering, Education, and Technology: “Education, Research and Leadership in Post-pandemic Engineering: Resilient, Inclusive and Sustainable Actions”The objective of this research was to develop a rapid method to identify and quantify chlorpyrifos and methamidophosin soils by Thin Layer Chromatography. A mobile phase of chloroform: acetone (80:20) was used for methamidophos and for chlorpyrifos a mixture of chloroform: cyclohexane (60:40) was used as mobile phase. The developer consisted of a 0.12 M ethanolic solution of silver nitrate. The stains were processed using "Image J" software. The results show retention factors "Rf" of 0.19 and 0.82 for methamidophos and chlorpyrifos respectively. Both methods for the determination of chlorpyrifos and methamidophos are linear with coefficients of determination R 2 greater than 0.99, precise with RSD less than 15 % and accurate with % R close to 100 % . The analysis of agricultural soil samples of Garlic and Onion showed the presence of chlorpyrifos with concentrations of 0.067 and 0.047 mg/kg respectively. Also, methamidophos was found in alfalfa agricultural soils with a concentration of 0.011 mg/kg. With the results found, it is demonstrated that image processing with "Image J" for the analysis of stains on silica gel plates developed with silver nitrate in the analysis of organophosphates can be taken into account for demonstrative studies for educational purposes and routine tests in toxicology and environment.Campus Arequipaapplication/pdfspaLatin American and Caribbean Consortium for Engineering InstitutionsPEProceedings of the LACCEI international Multi-conference for Engineering, Education and Technology;Vol. 2022-Julyinfo:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-sa/4.0/Repositorio Institucional - UTPUniversidad Tecnológica del Perúreponame:UTP-Institucionalinstname:Universidad Tecnológica del Perúinstacron:UTPSoilsChlorpyrifosMethamidophosThin Layer ChromatigraphyImage Processinghttps://purl.org/pe-repo/ocde/ford#2.11.04Development of a rapid method for the quantification of methamidophos and chlorpyrifos by Thin Layer Chromatography in soils using image processingDesarrollo de un método rápido para la cuantificación de metamidofos y clorpirifós por cromatografía en capa fina en suelos mediante procesamiento de imágenesinfo:eu-repo/semantics/conferenceObjectinfo:eu-repo/semantics/publishedVersionORIGINALDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdfDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdfapplication/pdf960237http://repositorio.utp.edu.pe/bitstream/20.500.12867/9807/1/Development-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf21781aa1765d0d3415839e4951e7edf4MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.utp.edu.pe/bitstream/20.500.12867/9807/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52TEXTDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.txtDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.txtExtracted texttext/plain33835http://repositorio.utp.edu.pe/bitstream/20.500.12867/9807/3/Development-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.txtb0457db0f43880d659e6735cffd6edc8MD53THUMBNAILDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.jpgDevelopment-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.jpgGenerated Thumbnailimage/jpeg15569http://repositorio.utp.edu.pe/bitstream/20.500.12867/9807/4/Development-of-a-rapid-method-for-the-quantification-of-methamidophos-and-chlorpyrifos-by-Thin-Layer-Chromatography-in-soils-using-image-processingProceedings-of-the-LACCEI-international-Multiconference-for-Enginee.pdf.jpg7961f441045307cb2b37e0243933653fMD5420.500.12867/9807oai:repositorio.utp.edu.pe:20.500.12867/98072024-10-01 03:06:56.663Repositorio Institucional de la Universidad Tecnológica del Perúrepositorio@utp.edu.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 |
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Nota importante:
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
La información contenida en este registro es de entera responsabilidad de la institución que gestiona el repositorio institucional donde esta contenido este documento o set de datos. El CONCYTEC no se hace responsable por los contenidos (publicaciones y/o datos) accesibles a través del Repositorio Nacional Digital de Ciencia, Tecnología e Innovación de Acceso Abierto (ALICIA).
