SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS

Descripción del Articulo

The N-Benzoyl-0-methyl - N1-(o-nitrophenyl)·isourea (L1) and N-Benzoyl-0-methyl·N1-(p-bromphenyl)-isourea (L2) ligands were slntheslzed by reactlon of the correspondlng N-Benzoyl-N1-phenyl-thioureas wlth mercury(II) acetate in methanolic solution. The characterlzation was made by elemental analysis,...

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Detalles Bibliográficos
Autores: Anaya M., Fernando, Beyer, Lothar, Sleler, J.
Formato: artículo
Fecha de Publicación:2001
Institución:Universidad Nacional Mayor de San Marcos
Repositorio:Revistas - Universidad Nacional Mayor de San Marcos
Lenguaje:español
OAI Identifier:oai:ojs.csi.unmsm:article/4279
Enlace del recurso:https://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279
Nivel de acceso:acceso abierto
Materia:N-Benzoyl-0-methyl-N1-phenyl isourea Ligands
X-ray structure
Ligandos N-Benzoil-O-metil-N1-fenil Isourea
Estructura de rayos X
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spelling SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREASSÍNTESIS Y CARACTERIZACIÓN DE LIGANDOS TIPO ISOUREASAnaya M., FernandoBeyer, LotharSleler, J.N-Benzoyl-0-methyl-N1-phenyl isourea LigandsX-ray structureLigandos N-Benzoil-O-metil-N1-fenil IsoureaEstructura de rayos XThe N-Benzoyl-0-methyl - N1-(o-nitrophenyl)·isourea (L1) and N-Benzoyl-0-methyl·N1-(p-bromphenyl)-isourea (L2) ligands were slntheslzed by reactlon of the correspondlng N-Benzoyl-N1-phenyl-thioureas wlth mercury(II) acetate in methanolic solution. The characterlzation was made by elemental analysis, hydrogen (1H) and carbon (13C) Nuclear Magnetic Resonance, mass spectroscopy and the measure of their physical properties. The crlitallyne molecular structure of (L1) was determined by X-ray dlfraction.Se han sintetizado los ligandos N-Benzoil-0-metil-N'-(o-nitrofenil)isourea (L1) y N-Benzoil-0-metil-N1-(p-bromofenil)isourea (L2) por reacción de los correspondientes ligandos N-Benzoil-N1-fenil tiourea con acetato de mercurio (II) en solución metanólica. La caracterización de estos productos se realizó mediante análisis elemental, resonancia magnético nuclear del hidrógeno (1H) y de carbono (13C), espectroscopia de masas y por medición de sus propiedades físicas. La estructura cristalina molecular de (L1) se determinó mediante difracción de rayos X.Universidad Nacional Mayor de San Marcos2001-12-31info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279Revista Peruana de Química e Ingeniería Química; Vol. 4 No. 2 (2001); 57-67Revista Peruana de Química e Ingeniería Química; Vol. 4 Núm. 2 (2001); 57-671609-75991726-2208reponame:Revistas - Universidad Nacional Mayor de San Marcosinstname:Universidad Nacional Mayor de San Marcosinstacron:UNMSMspahttps://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279/3418Derechos de autor 2001 Fernando Anaya M., Lothar Beyer, J. Slelerhttps://creativecommons.org/licenses/by-nc-sa/4.0info:eu-repo/semantics/openAccessoai:ojs.csi.unmsm:article/42792020-05-08T17:08:57Z
dc.title.none.fl_str_mv SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
SÍNTESIS Y CARACTERIZACIÓN DE LIGANDOS TIPO ISOUREAS
title SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
spellingShingle SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
Anaya M., Fernando
N-Benzoyl-0-methyl-N1-phenyl isourea Ligands
X-ray structure
Ligandos N-Benzoil-O-metil-N1-fenil Isourea
Estructura de rayos X
title_short SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
title_full SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
title_fullStr SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
title_full_unstemmed SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
title_sort SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
dc.creator.none.fl_str_mv Anaya M., Fernando
Beyer, Lothar
Sleler, J.
author Anaya M., Fernando
author_facet Anaya M., Fernando
Beyer, Lothar
Sleler, J.
author_role author
author2 Beyer, Lothar
Sleler, J.
author2_role author
author
dc.subject.none.fl_str_mv N-Benzoyl-0-methyl-N1-phenyl isourea Ligands
X-ray structure
Ligandos N-Benzoil-O-metil-N1-fenil Isourea
Estructura de rayos X
topic N-Benzoyl-0-methyl-N1-phenyl isourea Ligands
X-ray structure
Ligandos N-Benzoil-O-metil-N1-fenil Isourea
Estructura de rayos X
description The N-Benzoyl-0-methyl - N1-(o-nitrophenyl)·isourea (L1) and N-Benzoyl-0-methyl·N1-(p-bromphenyl)-isourea (L2) ligands were slntheslzed by reactlon of the correspondlng N-Benzoyl-N1-phenyl-thioureas wlth mercury(II) acetate in methanolic solution. The characterlzation was made by elemental analysis, hydrogen (1H) and carbon (13C) Nuclear Magnetic Resonance, mass spectroscopy and the measure of their physical properties. The crlitallyne molecular structure of (L1) was determined by X-ray dlfraction.
publishDate 2001
dc.date.none.fl_str_mv 2001-12-31
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv https://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279
url https://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279
dc.language.none.fl_str_mv spa
language spa
dc.relation.none.fl_str_mv https://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/4279/3418
dc.rights.none.fl_str_mv Derechos de autor 2001 Fernando Anaya M., Lothar Beyer, J. Sleler
https://creativecommons.org/licenses/by-nc-sa/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Derechos de autor 2001 Fernando Anaya M., Lothar Beyer, J. Sleler
https://creativecommons.org/licenses/by-nc-sa/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidad Nacional Mayor de San Marcos
publisher.none.fl_str_mv Universidad Nacional Mayor de San Marcos
dc.source.none.fl_str_mv Revista Peruana de Química e Ingeniería Química; Vol. 4 No. 2 (2001); 57-67
Revista Peruana de Química e Ingeniería Química; Vol. 4 Núm. 2 (2001); 57-67
1609-7599
1726-2208
reponame:Revistas - Universidad Nacional Mayor de San Marcos
instname:Universidad Nacional Mayor de San Marcos
instacron:UNMSM
instname_str Universidad Nacional Mayor de San Marcos
instacron_str UNMSM
institution UNMSM
reponame_str Revistas - Universidad Nacional Mayor de San Marcos
collection Revistas - Universidad Nacional Mayor de San Marcos
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 13.875689
SYNTHESIS and CHARACTERIZATION OF LIGAND TYPE ISOUREAS
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