Development and validation of a chromatographic method for the detection and quantification of Ivermectin residues in wastewater

• Autores: Colque-Ayma, Elvis Jack, Merma-Chacca, Donald Efrain, Ecos-Espino, Alejandro Manuel, Campos-Quiróz, Clara Nely, Ramos-Tejada, José Luis, Veja-Quispe, Anyela Pierina, Zirena-Vilca, Franz
• Formato: artículo
• Fecha de Publicación: 2023
• Institución: Universidad Nacional Intercultural Fabiola Salazar Leguía de Bagua
• Repositorio: Revistas - Universidad Nacional Intercultural Fabiola Salazar Leguía de Bagua
• Lenguaje: español
• OAI Identifier: oai:revista.unibagua.edu.pe:article/192
• Enlace del recurso: https://revista.unibagua.edu.pe/index.php/dekamuagropec/article/view/192
• Nivel de acceso: acceso abierto
• Materia: Validación, Antiparasitario, Ivermectina, Cromatógrafo, Cuantificación.; Validation, Antiparasitic, Ivermectin, Chromatograph, Quantification.

This study developed and validated a method of analysis by UHPL-DAD to detect and quantify Ivermectin (IVM) residues in wastewater. The implementation of this method consisted of a robust and efficient method, where the retention time for this residue was 3.1 min. However, the parameters considered in the validation process of the analytical method were: selectivity, linearity, detection limit, quantification limit and recovery percentage; the method is selective, the correlation coefficient is R2 ≥ 0.99, it presents a detection limit (LD) of 0.003 µg L-1, a quantification limit (LQ) of 0.01 µg L-1, and a recovery percentage of 90% (with fortification of 0.1 µg L-1).